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Arthashastra

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siva.sh/arthashastra/adhyaksa-pracara/14/9

तीक्ष्ण काकणी रूप्य द्वि गुणः राग प्रक्षेपः, तस्य षड् भागः क्षयः ॥

The colouring ingredient (rágaprakshépa) shall be two kákanis of tíkshna (copper sulphate ?) one-sixth of which will be lost during the manufacture.

english translation

Chapter 14

Verse 10